4UNA
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 2 DAYS INCUBATION IN 5MM MN (STATE 4)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 106.517, 70.153, 106.704 |
Unit cell angles | 90.00, 119.83, 90.00 |
Refinement procedure
Resolution | 46.285 - 2.300 |
R-factor | 0.1908 |
Rwork | 0.190 |
R-free | 0.21910 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs7 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.194 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.280 | 2.420 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.050 | 0.480 |
Number of reflections | 261170 | |
<I/σ(I)> | 16 | 2 |
Completeness [%] | 96.7 | 79.9 |
Redundancy | 4.4 | 3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | PH 6 |