4UN9
THE CRYSTAL STRUCTURE OF I-DMOI IN COMPLEX WITH ITS TARGET DNA AT 8H INCUBATION IN 5MM MN (STATE 3)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 6M |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 107.025, 70.657, 107.259 |
Unit cell angles | 90.00, 119.58, 90.00 |
Refinement procedure
Resolution | 42.860 - 2.734 |
R-factor | 0.1804 |
Rwork | 0.178 |
R-free | 0.21970 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2vs7 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.284 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((PHENIX.REFINE)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 46.650 | 2.850 |
High resolution limit [Å] | 2.730 | 2.730 |
Rmerge | 0.110 | 0.570 |
Number of reflections | 39637 | |
<I/σ(I)> | 10.5 | 2.3 |
Completeness [%] | 99.9 | 99.9 |
Redundancy | 4.7 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 6 | pH 6 |