4U70
HsMetAP (F309M) in complex with (1-amino-2-cyclohexylethyl)phosphonic acid
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2014-02-27 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.54 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 47.636, 77.389, 48.575 |
Unit cell angles | 90.00, 90.60, 90.00 |
Refinement procedure
Resolution | 17.090 - 1.600 |
R-factor | 0.166 |
Rwork | 0.164 |
R-free | 0.20700 |
RMSD bond length | 0.024 |
RMSD bond angle | 2.283 |
Data reduction software | XDS |
Data scaling software | SCALEPACK |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 18.000 |
High resolution limit [Å] | 1.600 |
Number of reflections | 46220 |
<I/σ(I)> | 2.57 |
Completeness [%] | 99.2 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6 | 298 | 15% PEGMME, 100mM HEPES PH 6. |