4U5J
C-Src in complex with Ruxolitinib
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 93 |
Detector technology | CCD |
Collection date | 2014-01-28 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.987 |
Spacegroup name | P 1 |
Unit cell lengths | 42.107, 63.228, 73.989 |
Unit cell angles | 79.27, 89.27, 90.29 |
Refinement procedure
Resolution | 43.398 - 2.260 |
R-factor | 0.1992 |
Rwork | 0.197 |
R-free | 0.23580 |
RMSD bond length | 0.009 |
RMSD bond angle | 1.273 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.260 |
Number of reflections | 34648 |
<I/σ(I)> | 15.9 |
Completeness [%] | 97.3 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | PEG 4000 |