4U58
IMPORTIN-ALPHA MINOR NLS SITE INHIBITOR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2011-11-05 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9686 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.160, 90.630, 101.030 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 62.311 - 2.560 |
R-factor | 0.2141 |
Rwork | 0.211 |
R-free | 0.26360 |
Data reduction software | XSCALE |
Refinement software | PHENIX ((phenix.refine: dev_1702)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 62.400 |
High resolution limit [Å] | 2.560 |
Number of reflections | 23793 |
<I/σ(I)> | 13.5 |
Completeness [%] | 97.5 |
Redundancy | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 291 | see publication |