4U1O
GluA2flip sLBD complexed with kainate and (R,R)-2b crystal form C
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 5.0.2 |
Synchrotron site | ALS |
Beamline | 5.0.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-01-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.0 |
Spacegroup name | P 21 21 2 |
Unit cell lengths | 57.310, 89.680, 48.660 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 42.770 - 1.850 |
R-factor | 0.169 |
Rwork | 0.167 |
R-free | 0.20900 |
RMSD bond length | 0.007 |
RMSD bond angle | 1.206 |
Data reduction software | XDS |
Refinement software | PHENIX ((PHENIX.REFINE: 1.8.2_1309)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 42.770 |
High resolution limit [Å] | 1.850 |
Number of reflections | 21890 |
<I/σ(I)> | 17.4 |
Completeness [%] | 99.1 |
Redundancy | 3.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M Na cacodylate, pH 6.5, 1.26 M ammonium sulfate |