4U1B

HsMetAP in complex with (1-amino-2-propylpentyl)phosphonic acid

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	IMAGE PLATE
Collection date	2014-03-20
Detector	RIGAKU RAXIS IV++
Wavelength(s)	1.54
Spacegroup name	P 1 21 1
Unit cell lengths	47.026, 76.929, 47.170
Unit cell angles	90.00, 92.39, 90.00

Refinement procedure

Resolution	20.000 - 1.890
R-factor	0.171
Rwork	0.169
R-free	0.22100
Phasing software	MOLREP
Refinement software	REFMAC

Data quality characteristics

	Overall
Low resolution limit [Å]	22.530
High resolution limit [Å]	1.890
Number of reflections	26171
<I/σ(I)>	3.16
Completeness [%]	98.0
Redundancy	3.6

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6	298	PEG 2000, potassium chloride, hepes, sodium chloride, pH 6.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K