4U17
Swapped dimer of the human Fyn-SH2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 1 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-07-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9801 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 88.965, 57.873, 101.188 |
Unit cell angles | 90.00, 90.60, 90.00 |
Refinement procedure
Resolution | 34.916 - 1.990 |
R-factor | 0.2093 |
Rwork | 0.207 |
R-free | 0.25540 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1g83 |
RMSD bond length | 0.012 |
RMSD bond angle | 1.413 |
Data reduction software | iMOSFLM |
Data scaling software | SCALA |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 34.920 | 2.100 |
High resolution limit [Å] | 1.990 | 1.990 |
Rmerge | 0.303 | |
Number of reflections | 35049 | |
<I/σ(I)> | 7.7 | 3.2 |
Completeness [%] | 98.7 | 98.9 |
Redundancy | 3.6 | 3.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 50 mM sodium phosphate pH 6.5 |