4U0Z
Eukaryotic Fic Domain containing protein with bound APCPP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I03 |
Synchrotron site | Diamond |
Beamline | I03 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-09-26 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.9763 |
Spacegroup name | P 1 |
Unit cell lengths | 77.100, 83.754, 130.023 |
Unit cell angles | 89.92, 89.57, 89.43 |
Refinement procedure
Resolution | 43.340 - 2.950 |
R-factor | 0.2082 |
Rwork | 0.206 |
R-free | 0.25110 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cuc |
RMSD bond length | 0.010 |
RMSD bond angle | 1.110 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 43.340 | 3.020 |
High resolution limit [Å] | 2.950 | 2.950 |
Rmerge | 0.496 | |
Number of reflections | 65073 | |
<I/σ(I)> | 4.4 | 1.7 |
Completeness [%] | 94.7 | |
Redundancy | 3.5 | 3.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 292 | 25% PEG 3350, 200mM Na K Tartrate, 100mM Bis-Tris Propane 7.5 |