4TV9
Tubulin-PM060184 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2013-03-03 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 1.00000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 104.200, 157.290, 180.220 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 52.044 - 2.000 |
R-factor | 0.1815 |
Rwork | 0.180 |
R-free | 0.20770 |
Structure solution method | FOURIER SYNTHESIS |
Starting model (for MR) | 4i4t |
RMSD bond length | 0.003 |
RMSD bond angle | 0.709 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 52.050 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.104 | |
Number of reflections | 199377 | |
<I/σ(I)> | 23.7 | 1.1 |
Completeness [%] | 99.9 | 99.1 |
Redundancy | 37.6 | 20.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.7 | 293 | 6% PEG, 16% glycerol, 30 mM magnesium chloride, 30 mM calcium chloride, 0.1M MES/0.1M imidazole |