4TT6
Crystal structure of ATAD2A bromodomain double mutant N1063A-Y1064A in apo form
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 8.3.1 |
Synchrotron site | ALS |
Beamline | 8.3.1 |
Temperature [K] | 193 |
Detector technology | CCD |
Collection date | 2013-08-09 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.11587 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 79.639, 79.639, 138.271 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 48.830 - 2.000 |
R-factor | 0.165 |
Rwork | 0.165 |
R-free | 0.17700 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3dai |
RMSD bond length | 0.012 |
RMSD bond angle | 1.360 |
Data scaling software | Aimless (0.1.27) |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 48.830 | 2.050 |
High resolution limit [Å] | 2.000 | 2.000 |
Rmerge | 0.111 | 0.713 |
Rpim | 0.018 | 0.112 |
Total number of observations | 746601 | 52818 |
Number of reflections | 18358 | |
<I/σ(I)> | 31.4 | 8.3 |
Completeness [%] | 100.0 | 100 |
Redundancy | 40.7 | 40.2 |
CC(1/2) | 0.999 | 0.978 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5.5 | 278 | 2.0M Ammonium sulfate, 0.1M Bis-Tris pH5.5 |