4TQ1

Crystal structure of human ATG5-TECAIR

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	PHOTON FACTORY BEAMLINE AR-NW12A
Synchrotron site	Photon Factory
Beamline	AR-NW12A
Temperature [K]	95
Detector technology	CCD
Collection date	2012-10-21
Detector	ADSC QUANTUM 210
Wavelength(s)	1
Spacegroup name	P 21 21 21
Unit cell lengths	43.618, 71.919, 96.354
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	34.780 - 1.802
R-factor	0.1811
Rwork	0.178
R-free	0.22240
RMSD bond length	0.007
RMSD bond angle	1.041
Refinement software	PHENIX ((phenix.refine: 1.8.2_1309))

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.800
Number of reflections	28746
<I/σ(I)>	34
Completeness [%]	100.0
Redundancy	7.8

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		277	MPD, PEG 1000, PEG 3350, alcohols, MES-imdazole