4TQ0
Crystal structure of human ATG5-ATG16N69
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | PHOTON FACTORY BEAMLINE AR-NW12A |
| Synchrotron site | Photon Factory |
| Beamline | AR-NW12A |
| Temperature [K] | 95 |
| Detector technology | CCD |
| Collection date | 2012-03-06 |
| Detector | ADSC QUANTUM 210 |
| Wavelength(s) | 1 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 93.094, 93.094, 245.577 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 37.092 - 2.697 |
| R-factor | 0.2074 |
| Rwork | 0.203 |
| R-free | 0.27420 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.390 |
| Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 50.000 |
| High resolution limit [Å] | 2.697 |
| Number of reflections | 28321 |
| <I/σ(I)> | 39.1 |
| Completeness [%] | 99.9 |
| Redundancy | 15.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 400, MgCl2, KCl, Tris-HCl |
