4TM4
Kutzneria sp. 744 ornithine N-hydroxylase, KtzI-FADox-red-NADP+-Br
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 24-ID-C |
Synchrotron site | APS |
Beamline | 24-ID-C |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2012-12-10 |
Detector | PSI PILATUS 6M |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 82.387, 151.956, 163.551 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 46.122 - 2.632 |
R-factor | 0.1945 |
Rwork | 0.193 |
R-free | 0.22340 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3s5w |
RMSD bond length | 0.015 |
RMSD bond angle | 1.622 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.9_1692)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.680 |
High resolution limit [Å] | 2.630 | 2.630 |
Number of reflections | 61333 | |
<I/σ(I)> | 14.8 | 2.4 |
Completeness [%] | 99.2 | 99.3 |
Redundancy | 4.9 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 298 | 0.9-1.2 M sodium bromide, 22-25% PEG 3350, 0.1 M Bis-tris propane pH 7.5 |