4TL8
Crystal structure of N-terminal C1 domain of KaiC
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL44XU |
Synchrotron site | SPring-8 |
Beamline | BL44XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-01-23 |
Detector | RAYONIX MX225HE |
Wavelength(s) | 0.9 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 79.934, 133.215, 150.706 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 37.591 - 1.859 |
R-factor | 0.1826 |
Rwork | 0.180 |
R-free | 0.22200 |
Starting model (for MR) | 2gbl |
RMSD bond length | 0.014 |
RMSD bond angle | 1.486 |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.520 |
High resolution limit [Å] | 1.859 |
Number of reflections | 132647 |
<I/σ(I)> | 48 |
Completeness [%] | 97.8 |
Redundancy | 7.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 293.15 | PEG 400 or PEG 8000 |