4TK0
Crystal Structure of human Tankyrase 2 in complex with DPQ.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 17-ID |
Synchrotron site | APS |
Beamline | 17-ID |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2009-08-12 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 1.000 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 74.040, 79.570, 153.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 76.820 - 1.650 |
R-factor | 0.1878 |
Rwork | 0.187 |
R-free | 0.22500 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.060 |
Data reduction software | XDS (2005/3) |
Refinement software | BUSTER-TNT (BUSTER 2.10.0) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 79.570 | 79.570 | 1.670 |
High resolution limit [Å] | 1.650 | 4.710 | 1.650 |
Rmerge | 0.062 | 0.029 | 0.602 |
Total number of observations | 709713 | ||
Number of reflections | 101327 | 5079 | 1416 |
<I/σ(I)> | 18.45 | 55.03 | 1.81 |
Completeness [%] | 92.4 | 99.5 | 77.6 |
Redundancy | 6.47 | 6.78 | 3.57 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 293 | 0.2M NaCl, 0.1M Sodium, Hepes buffer at pH7.5, 12-15% iso-propanol |