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4RSS

Crystal structure of tyrosine-protein kinase SYK with an inhibitor

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsSPRING-8 BEAMLINE BL44XU
Synchrotron siteSPring-8
BeamlineBL44XU
Temperature [K]100
Detector technologyCCD
Collection date2011-06-29
DetectorADSC QUANTUM 315r
Wavelength(s)1.0000
Spacegroup nameP 1 21 1
Unit cell lengths39.964, 88.281, 40.850
Unit cell angles90.00, 91.48, 90.00
Refinement procedure
Resolution44.140 - 1.830
R-factor0.21375
Rwork0.212
R-free0.24869
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.011
RMSD bond angle1.480
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwareMOLREP
Refinement softwareREFMAC (5.8.0049)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]50.0001.860
High resolution limit [Å]1.8301.830
Number of reflections24171
Completeness [%]97.097.6
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP8.527710-20% (v/v) PEG 3350, 100mM Tris-HCl (pH 8.5) , VAPOR DIFFUSION, HANGING DROP, temperature 277K

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