4RN5
B1 domain of human Neuropilin-1 with acetate ion in a ligand-binding site
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RU200 |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2009-12-01 |
Detector | RIGAKU RAXIS IV |
Wavelength(s) | 1.5418 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.839, 62.839, 87.918 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 21.540 - 1.730 |
R-factor | 0.1776 |
Rwork | 0.176 |
R-free | 0.20080 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.013 |
RMSD bond angle | 1.384 |
Data reduction software | d*TREK |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 21.540 | 1.840 |
High resolution limit [Å] | 1.730 | 1.730 |
Number of reflections | 16198 | |
Completeness [%] | 84.9 | 31 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 6 | 293 | 100mM MES, 200mM Zinc Acetate, 10% PEG 8000, pH 6.0, VAPOR DIFFUSION, temperature 293K |