4RAK

Crystal structure of nuclear receptor subfamily 1, group h, member 2 (lxrb) complexed with partial agonist

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SSRL BEAMLINE BL9-1
Synchrotron site	SSRL
Beamline	BL9-1
Detector technology	CCD
Detector	ADSC QUANTUM 315r
Wavelength(s)	0.979
Spacegroup name	I 21 21 21
Unit cell lengths	55.820, 120.630, 176.250
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	53.210 - 2.040
R-factor	0.23159
Rwork	0.229
R-free	0.27068
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	1.642
Refinement software	REFMAC (5.2.0019)

Data quality characteristics

	Overall
Low resolution limit [Å]	50.000
High resolution limit [Å]	1.950
Number of reflections	38284
Completeness [%]	87.2
Redundancy	6.4

Crystallization Conditions

crystal ID	method	pH	temperature	details
1