4QMD
Crystal structure of human envoplakin plakin repeat domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-09-16 |
Detector | RIGAKU SATURN 944 |
Wavelength(s) | 1.5417 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 42.480, 68.950, 112.200 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 19.974 - 1.601 |
R-factor | 0.172 |
Rwork | 0.168 |
R-free | 0.20460 |
Structure solution method | SAD |
RMSD bond length | 0.006 |
RMSD bond angle | 1.018 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | SOLVE |
Refinement software | PHENIX (1.7.1_743) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 19.974 | 4.680 | 1.700 |
High resolution limit [Å] | 1.600 | 3.360 | 1.600 |
Rmerge | 0.058 | 0.031 | 0.385 |
Number of reflections | 5740 | 9413 | |
<I/σ(I)> | 27.9 | 95.66 | 2.09 |
Completeness [%] | 92.9 | 100 | 67.2 |
Redundancy | 6.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 298 | 20% PEG 3350, 0.1M BIS Tris-CL, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |