4QGZ

X-ray structure of the adduct formed between hen egg white lysozyme and trans-dimethylamine methylamine dichlorido platinum(II)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Detector	RIGAKU SATURN 944+
Wavelength(s)	1.5418
Spacegroup name	P 43 21 2
Unit cell lengths	77.920, 77.920, 36.921
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	55.100 - 2.510
R-factor	0.18302
Rwork	0.179
R-free	0.25886
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.453
Data reduction software	HKL-2000
Data scaling software	HKL-2000
Phasing software	PHASER
Refinement software	REFMAC (5.8.0049)

Data quality characteristics

	Overall
Low resolution limit [Å]	55.100
High resolution limit [Å]	2.510
Number of reflections	4246
Completeness [%]	100.0

Crystallization Conditions

crystal ID	method	pH	temperature	details
1