4Q3F
Human D-DT complexed with tartrate
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | Cu FINE FOCUS |
| Temperature [K] | 200 |
| Detector technology | IMAGE PLATE |
| Collection date | 2014-03-18 |
| Detector | RIGAKU RAXIS IV++ |
| Wavelength(s) | 1.5418 |
| Spacegroup name | P 3 |
| Unit cell lengths | 83.730, 83.730, 40.560 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 29.130 - 1.800 |
| R-factor | 0.14639 |
| Rwork | 0.144 |
| R-free | 0.19827 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.019 |
| RMSD bond angle | 1.769 |
| Data reduction software | MOSFLM |
| Data scaling software | SCALA |
| Refinement software | REFMAC (5.8.0069) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 29.130 |
| High resolution limit [Å] | 1.800 |
| Number of reflections | 27672 |
| Completeness [%] | 93.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7.3 | 295 | 0.2 M Sodium tartrate dibasic dihydrate and 20% w/v Polyethylene glycol 3,350, pH 7.3, VAPOR DIFFUSION, HANGING DROP, temperature 295K |
