4PZG
Crystal structure of human sorting nexin 10 (SNX10)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Detector technology | CCD |
Collection date | 2014-03-13 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.9792 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 205.859, 205.859, 42.330 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 49.450 - 2.800 |
R-factor | 0.1966 |
Rwork | 0.194 |
R-free | 0.23700 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.019 |
RMSD bond angle | 1.970 |
Data scaling software | Aimless (0.1.29) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.450 | 49.450 | 2.950 |
High resolution limit [Å] | 2.800 | 8.850 | 2.800 |
Rmerge | 0.136 | 0.043 | 0.674 |
Total number of observations | 8982 | 13007 | |
Number of reflections | 25144 | ||
<I/σ(I)> | 10.5 | 27.2 | 2.2 |
Completeness [%] | 98.7 | 99.5 | 94.6 |
Redundancy | 6.5 | 10.5 | 3.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION | 7 | 293 | 4 M sodium nitrate, 0.1 M BIS-TRIS propane pH 7.0, vapor diffusion, temperature 293K |