4PJ9
Structure of human MR1-5-OP-RU in complex with human MAIT TRAJ20 TCR
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-08-21 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 111.560, 111.560, 204.150 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.730 - 2.000 |
R-factor | 0.1738 |
Rwork | 0.172 |
R-free | 0.19920 |
RMSD bond length | 0.010 |
RMSD bond angle | 1.000 |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 40.000 |
High resolution limit [Å] | 2.000 |
Number of reflections | 89271 |
<I/σ(I)> | 9.6 |
Completeness [%] | 100.0 |
Redundancy | 7 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 293 | PEG 3350, Bis-tris propane, sodium acetate |