4PDC
Crystal structure of Cowpox virus CPXV018 (OMCP) bound to human NKG2D
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-10-19 |
Detector | NOIR-1 |
Wavelength(s) | 1.00004 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.315, 101.110, 91.368 |
Unit cell angles | 90.00, 91.63, 90.00 |
Refinement procedure
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 50.000 | 50.000 | 2.070 |
High resolution limit [Å] | 1.991 | 4.310 | 2.000 |
Rmerge | 0.118 | 0.073 | 0.485 |
Total number of observations | 309692 | ||
Number of reflections | 50139 | ||
<I/σ(I)> | 12.7 | ||
Completeness [%] | 93.5 | 99.9 | 91.5 |
Redundancy | 6.2 | 7.6 | 5.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.75 | 293 | 15% PEG 3350, 0.2M MgCl2, 0.1M Bis-Tris |