4PC6
Elongation factor Tu:Ts complex with bound GDPNP
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ELETTRA BEAMLINE 5.2R |
Synchrotron site | ELETTRA |
Beamline | 5.2R |
Temperature [K] | 292 |
Detector technology | CCD |
Collection date | 2002-10-17 |
Detector | MAR CCD 165 mm |
Wavelength(s) | 1.2 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 73.969, 107.467, 193.339 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 29.542 - 2.200 |
R-factor | 0.173 |
Rwork | 0.171 |
R-free | 0.22310 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4pc1 |
RMSD bond length | 0.004 |
RMSD bond angle | 0.809 |
Refinement software | PHENIX ((phenix.refine: dev_1702)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 29.600 | 2.280 |
High resolution limit [Å] | 2.200 | 2.200 |
Rmerge | 0.010 | 0.440 |
Number of reflections | 79003 | |
<I/σ(I)> | 13.8 | 3.4 |
Completeness [%] | 99.5 | 98.5 |
Redundancy | 7.7 | 4.4 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 292 | 100mM MES, 18% PEG 6000, 5% glycerol, 152mM NH4CH3COO, 0.5mM GDPNP, 0.5mM pulvomycin, 5mM EDTA |