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4P65

Crystal structure of an cyclohexylalanine substituted insulin analog.

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 19-ID
Synchrotron siteAPS
Beamline19-ID
Temperature [K]100
Detector technologyCCD
Collection date2012-06-13
DetectorADSC QUANTUM 315r
Wavelength(s)0.987
Spacegroup nameP 1 21 1
Unit cell lengths46.040, 60.900, 59.300
Unit cell angles90.00, 112.25, 90.00
Refinement procedure
Resolution42.300 - 1.500
R-factor0.1641
Rwork0.160
R-free0.20260
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)1znj
RMSD bond length0.010
RMSD bond angle1.351
Refinement softwarePHENIX ((phenix.refine: 1.9_1692))
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]42.3001.600
High resolution limit [Å]1.5001.500
Rmerge0.840
Number of reflections54128
<I/σ(I)>13.91.6
Completeness [%]95.899.3
Redundancy1.93.5
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, HANGING DROP277sodium citrate, phenol, sodium chloride, zinc acetate, tris

217705

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