4P57

MHC TCR peptide complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	APS BEAMLINE 24-ID-C
Synchrotron site	APS
Beamline	24-ID-C
Temperature [K]	273
Detector technology	PIXEL
Collection date	2013-03-23
Detector	PSI PILATUS 6M
Wavelength(s)	1
Spacegroup name	P 41 21 2
Unit cell lengths	102.392, 102.392, 234.330
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	77.100 - 2.600
R-factor	0.21
Rwork	0.208
R-free	0.24500
RMSD bond length	0.010
RMSD bond angle	1.350
Refinement software	BUSTER (2.10.0)

Data quality characteristics

	Overall
Low resolution limit [Å]	90.000
High resolution limit [Å]	2.600
Number of reflections	37601
<I/σ(I)>	10
Completeness [%]	93.9
Redundancy	2.3

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		293	Ca acetate, tris, PEG300