4P4S
GMPPCP-bound stalkless-MxA
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX2 |
Synchrotron site | Australian Synchrotron |
Beamline | MX2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-10-04 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.95 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 60.290, 66.760, 170.840 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.260 - 3.300 |
R-factor | 0.23441 |
Rwork | 0.231 |
R-free | 0.30531 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4p4u |
RMSD bond length | 0.012 |
RMSD bond angle | 1.605 |
Refinement software | REFMAC (5.8.0049) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 49.260 | 3.400 |
High resolution limit [Å] | 3.300 | 3.300 |
Number of reflections | 10950 | |
<I/σ(I)> | 19 | 2.9 |
Completeness [%] | 99.9 | 100 |
Redundancy | 9 | 9.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.9 | 291 | 23-27% PEG 4000, 0.2 M EPPS/KOH pH 7.9, 0.5M glycerol |