4OYE
Crystal structure of GltPh R397A in apo
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X29A |
| Synchrotron site | NSLS |
| Beamline | X29A |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2013-07-19 |
| Detector | ADSC QUANTUM 315r |
| Wavelength(s) | 0.9700 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 112.365, 424.422, 113.985 |
| Unit cell angles | 90.00, 119.38, 90.00 |
Refinement procedure
| Resolution | 20.000 - 4.000 |
| R-factor | 0.24993 |
| Rwork | 0.249 |
| R-free | 0.26648 |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.393 |
| Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
| Overall | |
| Low resolution limit [Å] | 20.000 |
| High resolution limit [Å] | 4.000 |
| Number of reflections | 52068 |
| <I/σ(I)> | 12.3 |
| Completeness [%] | 70.3 |
| Redundancy | 2 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 277 | PEG400 Choline chloride citrate/tris |
