4OUF
Crystal Structure of CBP bromodomain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALS BEAMLINE 4.2.2 |
Synchrotron site | ALS |
Beamline | 4.2.2 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-04-14 |
Detector | NOIR-1 |
Wavelength(s) | 1.0 |
Spacegroup name | H 3 |
Unit cell lengths | 121.790, 121.790, 40.710 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 35.158 - 1.400 |
R-factor | 0.1509 |
Rwork | 0.149 |
R-free | 0.19100 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 2g3r |
RMSD bond length | 0.009 |
RMSD bond angle | 1.253 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.4_1496)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 35.160 | 1.450 |
High resolution limit [Å] | 1.400 | 1.400 |
Rmerge | 0.080 | 0.245 |
Number of reflections | 44684 | |
<I/σ(I)> | 10.7 | 3 |
Completeness [%] | 98.8 | 90.9 |
Redundancy | 5.21 | 2.95 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 277 | 0.1 M HEPES-Na pH 7.0, 0.2M KSCN, 25% PEG3350 and 5% Ethylene Glycol, VAPOR DIFFUSION, HANGING DROP, temperature 277K |