Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS BEAMLINE X8C |
| Synchrotron site | NSLS |
| Beamline | X8C |
| Temperature [K] | 100 |
| Detector technology | CCD |
| Collection date | 2001-04-12 |
| Detector | ADSC QUANTUM 4 |
| Wavelength(s) | 1.005 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 72.620, 140.430, 145.850 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 28.487 - 2.000 |
| R-factor | 0.1893 |
| Rwork | 0.186 |
| R-free | 0.21860 |
| Structure solution method | MIR |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.071 |
| Data reduction software | DENZO |
| Data scaling software | SCALEPACK |
| Phasing software | MLPHARE |
| Refinement software | PHENIX (1.8_1069) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 28.487 | 2.250 |
| High resolution limit [Å] | 2.000 | 2.000 |
| Rmerge | 0.400 | |
| Number of reflections | 50208 | |
| <I/σ(I)> | 20.1 | 2.7 |
| Completeness [%] | 99.0 | 97.9 |
| Redundancy | 5.8 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6 | 298 | PEG 4000, SODIUM CITRATE, pH 6.0, VAPOR DIFFUSION, temperature 298K |
