4NXP
Crystal Structure of Free T-cell Lymphoma Invasion and Metastasis-1 PDZ Domain Quadruple Mutant (QM)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU RUH3R |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2011-07-21 |
Detector | RIGAKU RAXIS IV++ |
Wavelength(s) | 1.5418 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 45.843, 45.843, 71.362 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 19.850 - 2.300 |
R-factor | 0.21873 |
Rwork | 0.217 |
R-free | 0.25777 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3kzd |
RMSD bond length | 0.005 |
RMSD bond angle | 1.098 |
Data reduction software | d*TREK |
Data scaling software | d*TREK |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0032) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 19.850 | 2.380 |
High resolution limit [Å] | 2.300 | 2.300 |
Rmerge | 0.104 | 0.421 |
Number of reflections | 3866 | |
<I/σ(I)> | 7.7 | 2.1 |
Completeness [%] | 93.9 | 97.3 |
Redundancy | 3.18 | 3.17 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 6.8 | 291 | 1.5M Ammonium Sulfate, 0.1M Tris, pH=8.5, 12% Glycerol, pH 6.8, VAPOR DIFFUSION, HANGING DROP, temperature 291K |