Loading
PDBj
MenuPDBj@FacebookPDBj@TwitterPDBj@YouTubewwPDB FoundationwwPDB
RCSB PDBPDBeBMRBAdv. SearchSearch help

4NRC

Crystal Structure of the bromodomain of human BAZ2B in complex with compound-3 N01186

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeROTATING ANODE
Source detailsRIGAKU FR-E SUPERBRIGHT
Temperature [K]100
Detector technologyIMAGE PLATE
Collection date2011-01-30
DetectorRIGAKU RAXIS IV
Wavelength(s)1.5418
Spacegroup nameC 2 2 21
Unit cell lengths81.270, 96.590, 57.740
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution28.870 - 1.860
R-factor0.1735
Rwork0.173
R-free0.19060
Structure solution methodMOLECULAR REPLACEMENT
Starting model (for MR)3g0l
RMSD bond length0.010
RMSD bond angle0.870
Data reduction softwareMOSFLM
Data scaling softwareSCALA
Phasing softwarePHASER
Refinement softwareBUSTER (2.8.0)
Data quality characteristics
 OverallOuter shell
Low resolution limit [Å]29.9301.960
High resolution limit [Å]1.8601.860
Rmerge0.0930.802
Number of reflections19430
<I/σ(I)>13.72
Completeness [%]100.0100
Redundancy5.15
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION, SITTING DROP7.5277.1519% PEG 1000, 12% glycerol, pH 7.5, VAPOR DIFFUSION, SITTING DROP, temperature 277.15K

227111

PDB entries from 2024-11-06

PDB statisticsPDBj update infoContact PDBjnumon