4NNI
Structural basis for targeting the ribosomal protein S1 of Mycobacterium tuberculosis by pyrazinamide
Experimental procedure
Experimental method | MAD |
Source type | SYNCHROTRON |
Source details | OTHER |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-04-25 |
Detector | RAYONIX MX-225 |
Wavelength(s) | 0.979 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 66.506, 66.593, 127.162 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 32.230 - 2.640 |
R-factor | 0.21586 |
Rwork | 0.214 |
R-free | 0.25525 |
Structure solution method | MAD |
RMSD bond length | 0.015 |
RMSD bond angle | 1.539 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER (2.3.0) |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 2.600 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | hanging drop | 8 | 295 | PEG 3350, pH 8.0, hanging drop, temperature 295K |