4NHT
X-ray structure of the complex between hen egg white lysozyme and pentachlorocarbonyliridate(III) (6 days)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | RIGAKU MICROMAX-007 HF |
Temperature [K] | 100 |
Collection date | 2012-10-11 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 78.583, 78.583, 37.118 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.520 - 1.650 |
R-factor | 0.2121 |
Rwork | 0.199 |
R-free | 0.22790 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | CNS |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 55.567 |
High resolution limit [Å] | 1.650 |
Number of reflections | 14522 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 4.5 | 298 | Ir(Cl)5CO for 6 days, pH 4.5, VAPOR DIFFUSION, HANGING DROP, temperature 298K |