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4NF6

Crystal structure of GluN1/GluN2A ligand-binding domain in complex with glycine and PPDA

Experimental procedure
Experimental methodSINGLE WAVELENGTH
Source typeSYNCHROTRON
Source detailsAPS BEAMLINE 23-ID-B
Synchrotron siteAPS
Beamline23-ID-B
Temperature [K]100
Detector technologyCCD
Collection date2012-01-01
DetectorADSC QUANTUM 315
Wavelength(s)1.0
Spacegroup nameP 21 21 21
Unit cell lengths59.542, 84.690, 122.799
Unit cell angles90.00, 90.00, 90.00
Refinement procedure
Resolution19.949 - 2.100
R-factor0.1661
Rwork0.164
R-free0.21460
Structure solution methodMOLECULAR REPLACEMENT
RMSD bond length0.007
RMSD bond angle1.047
Data reduction softwareHKL-2000
Data scaling softwareHKL-2000
Phasing softwarePHASER
Refinement softwarePHENIX ((phenix.refine: 1.8.1_1168))
Data quality characteristics
 Overall
Low resolution limit [Å]50.000
High resolution limit [Å]2.100
Number of reflections36421
Completeness [%]98.4
Crystallization Conditions
crystal IDmethodpHtemperaturedetails
1VAPOR DIFFUSION7300PEG2000MMG and HEPES, pH 7, VAPOR DIFFUSION, temperature 300K

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