4N43
Human enterovirus 71 uncoating intermediate captured at atomic resolution
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-07-03 |
Detector | ADSC QUANTUM 315 |
Wavelength(s) | 0.97914 |
Spacegroup name | P 42 3 2 |
Unit cell lengths | 352.416, 352.416, 352.416 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 49.840 - 3.801 |
R-factor | 0.2466 |
Rwork | 0.245 |
R-free | 0.27410 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1pov |
RMSD bond length | 0.002 |
RMSD bond angle | 0.641 |
Data reduction software | DENZO |
Data scaling software | SCALEPACK |
Phasing software | PHASER |
Refinement software | PHENIX |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 49.840 | 50.000 | 3.870 |
High resolution limit [Å] | 3.801 | 10.290 | 3.801 |
Rmerge | 0.384 | 0.170 | 0.839 |
Number of reflections | 50069 | ||
<I/σ(I)> | 2.3 | 19.48 | 1.34 |
Completeness [%] | 68.0 | 56.1 | 73.4 |
Redundancy | 5 | 5.6 | 4.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 7 | 289 | 0.1M Cacodylate containing 1.6M Sodium Acetate, pH 7.0, vapor diffusion, hanging drop, temperature 289K |