4MZV
Crystal structure of extracellular part of human EpCAM
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | BRUKER AXS MICROSTAR |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2010-02-02 |
Detector | Bruker Platinum 135 |
Wavelength(s) | 1.542 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 88.022, 50.385, 67.828 |
Unit cell angles | 90.00, 128.33, 90.00 |
Refinement procedure
Resolution | 27.790 - 1.865 |
R-factor | 0.1965 |
Rwork | 0.194 |
R-free | 0.24910 |
Structure solution method | SAD |
RMSD bond length | 0.010 |
RMSD bond angle | 1.273 |
Data reduction software | PROTEUM2 |
Data scaling software | PROTEUM2 |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.8.1_1168)) |
Data quality characteristics
Overall | Inner shell | Outer shell | |
Low resolution limit [Å] | 27.794 | 27.790 | 1.910 |
High resolution limit [Å] | 1.860 | 5.060 | 1.860 |
Number of reflections | 18527 | ||
<I/σ(I)> | 33.98 | 86.54 | 2.6 |
Completeness [%] | 99.2 | 99.6 | 85.5 |
Redundancy | 26.6 | 46.19 | 6.33 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 293 | 0.2M magnesium chloride, 0.1M TRIS-HCl, 30% w/v PEG 4000, 0.16 mM decyl-beta-D-maltopyranoside, pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 293K |