Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | AUSTRALIAN SYNCHROTRON BEAMLINE MX1 |
Synchrotron site | Australian Synchrotron |
Beamline | MX1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-12-14 |
Detector | ADSC QUANTUM 210r |
Wavelength(s) | 0.953693 |
Spacegroup name | P 21 21 21 |
Unit cell lengths | 78.033, 89.948, 99.440 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 38.966 - 1.880 |
R-factor | 0.175 |
Rwork | 0.174 |
R-free | 0.19510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.015 |
RMSD bond angle | 1.496 |
Data reduction software | XDS |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 99.440 | 1.980 |
High resolution limit [Å] | 1.880 | 1.880 |
Number of reflections | 57564 | |
Completeness [%] | 99.9 | 100 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | Sodium citrate, DTT, pH 7, VAPOR DIFFUSION, HANGING DROP, temperature 293K |