4MTC
Crystal structure of human C53A DJ-1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2011-01-01 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.378 |
Spacegroup name | P 31 2 1 |
Unit cell lengths | 75.220, 75.220, 75.640 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 24.680 - 1.470 |
R-factor | 0.1601 |
Rwork | 0.160 |
R-free | 0.16500 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 1.124 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER ((2.1.2)) |
Refinement software | PHENIX ((phenix.refine: 1.6.1_357)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 37.820 | 1.550 |
High resolution limit [Å] | 1.470 | 1.470 |
Rmerge | 0.096 | 0.419 |
Number of reflections | 42517 | |
Completeness [%] | 99.6 | 99.9 |
Redundancy | 10.3 | 10.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 8 | 293 | 0.2 M Sodium Malonate, 20% w/v PEG 3350, pH 8, VAPOR DIFFUSION, HANGING DROP, temperature 293K |