4MMU
Crystal Structure of Prefusion-stabilized RSV F Variant DS-Cav1 at pH 5.5
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | APS BEAMLINE 22-ID |
Synchrotron site | APS |
Beamline | 22-ID |
Temperature [K] | 100 |
Detector technology | IMAGE PLATE |
Collection date | 2013-06-02 |
Detector | MAR scanner 300 mm plate |
Spacegroup name | P 41 3 2 |
Unit cell lengths | 168.588, 168.588, 168.588 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 28.500 - 3.000 |
R-factor | 0.181 |
Rwork | 0.178 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 4jhw |
RMSD bond length | 0.010 |
RMSD bond angle | 1.430 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | BUSTER (2.10.0) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 50.000 |
High resolution limit [Å] | 3.000 |
Rmerge | 0.220 |
Number of reflections | 16922 |
<I/σ(I)> | 22.4 |
Completeness [%] | 99.8 |
Redundancy | 16.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | 5.5 | 1.8 M Ammonium sulphate 0.1 M citrate pH5.5, VAPOR DIFFUSION, HANGING DROP |