4ML0
Crystal structure of E.coli DinJ-YafQ complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-01-03 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.9792 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 175.901, 120.250, 120.201 |
Unit cell angles | 90.00, 130.40, 90.00 |
Refinement procedure
Resolution | 43.713 - 2.100 |
R-factor | 0.1748 |
Rwork | 0.175 |
R-free | 0.21510 |
Structure solution method | SAD |
RMSD bond length | 0.008 |
RMSD bond angle | 1.063 |
Data reduction software | HKL-2000 |
Data scaling software | SCALEPACK |
Phasing software | SOLVE |
Refinement software | PHENIX ((phenix.refine: 1.7.3_928)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.140 |
High resolution limit [Å] | 2.100 | 2.100 |
Rmerge | 0.102 | 0.458 |
Number of reflections | 110921 | |
<I/σ(I)> | 33 | 9.32 |
Completeness [%] | 99.2 | 100 |
Redundancy | 4.9 | 5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 2M (NH4)2SO4, 2.5% 2-Propanol, pH 7.0, VAPOR DIFFUSION, HANGING DROP, temperature 293K |