4MGZ
Selective activation of Epac1 and Epac2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ESRF BEAMLINE ID23-1 |
Synchrotron site | ESRF |
Beamline | ID23-1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2008-11-02 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 1.07225 |
Spacegroup name | I 21 21 21 |
Unit cell lengths | 125.228, 147.088, 226.740 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 35.850 - 3.000 |
R-factor | 0.23963 |
Rwork | 0.238 |
R-free | 0.26435 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3cf6 |
RMSD bond length | 0.006 |
RMSD bond angle | 1.041 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | MOLREP |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.000 | 3.100 |
High resolution limit [Å] | 3.000 | 3.000 |
Number of reflections | 41504 | |
<I/σ(I)> | 4.6 | |
Completeness [%] | 98.2 | 99.6 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 5.6 | 277 | 0.4M (NH4)2SO4, 1.2M LI2SO4, 0.1M CITRATE, pH 5.6, VAPOR DIFFUSION, SITTING DROP, temperature 277K |