4M9R
Crystal structure of CED-3
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | CHESS BEAMLINE A1 |
Synchrotron site | CHESS |
Beamline | A1 |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2005-11-30 |
Detector | ADSC QUANTUM 210 |
Wavelength(s) | 0.987 |
Spacegroup name | I 41 |
Unit cell lengths | 121.070, 121.070, 58.470 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 20.178 - 2.656 |
R-factor | 0.2088 |
Rwork | 0.206 |
R-free | 0.26030 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 1cp3 |
RMSD bond length | 0.005 |
RMSD bond angle | 0.834 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 20.178 | 2.920 |
High resolution limit [Å] | 2.650 | 2.650 |
Number of reflections | 11999 | |
Completeness [%] | 97.0 | 89.1 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 7.5 | 295 | 0.1M HEPES, 20%(w/v) PEG3350, 0.2M (NH4)2SO4 , pH 7.5, VAPOR DIFFUSION, HANGING DROP, temperature 295K |