4LN0
Crystal structure of the VGLL4-TEAD4 complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U |
Synchrotron site | SSRF |
Beamline | BL17U |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2013-01-22 |
Detector | ADSC QUANTUM 315r |
Wavelength(s) | 0.97915 |
Spacegroup name | P 32 2 1 |
Unit cell lengths | 94.817, 94.817, 135.172 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 41.057 - 2.896 |
R-factor | 0.1918 |
Rwork | 0.185 |
R-free | 0.24710 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | 3jua |
RMSD bond length | 0.009 |
RMSD bond angle | 1.261 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX ((phenix.refine: 1.8.2_1309)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.950 |
High resolution limit [Å] | 2.896 | 2.900 |
Rmerge | 0.164 | 0.942 |
Number of reflections | 15590 | |
<I/σ(I)> | 15.86 | 5.28 |
Completeness [%] | 96.5 | 97.6 |
Redundancy | 5.5 | 5.5 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 289 | 0.2M L-proline, 0.1M HEPES pH 7.5, 24% PEG 1500, VAPOR DIFFUSION, SITTING DROP, temperature 289K |