4LMF
C1s CUB1-EGF-CUB2
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I04-1 |
Synchrotron site | Diamond |
Beamline | I04-1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Detector | DECTRIS PILATUS 2M |
Wavelength(s) | 0.98 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 67.876, 71.668, 157.723 |
Unit cell angles | 90.00, 95.93, 90.00 |
Refinement procedure
Resolution | 67.510 - 2.921 |
R-factor | 0.2106 |
Rwork | 0.208 |
R-free | 0.25210 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 0.773 |
Data reduction software | MOSFLM |
Data scaling software | SCALA |
Phasing software | PHASER |
Refinement software | PHENIX (1.8.2_1309) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 67.510 | 3.000 |
High resolution limit [Å] | 2.920 | 2.920 |
Number of reflections | 32566 | |
Completeness [%] | 98.9 | 91 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8.5 | 298 | pH 8.5, VAPOR DIFFUSION, SITTING DROP, temperature 298K |