4LL4
The structure of the TRX and TXNIP complex
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PAL/PLS BEAMLINE 5C (4A) |
Synchrotron site | PAL/PLS |
Beamline | 5C (4A) |
Temperature [K] | 173.15 |
Detector technology | CCD |
Collection date | 2009-07-27 |
Wavelength(s) | 1.100 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 79.826, 64.990, 88.416 |
Unit cell angles | 90.00, 90.88, 90.00 |
Refinement procedure
Resolution | 40.000 - 2.700 |
R-factor | 0.2013 |
Rwork | 0.196 |
R-free | 0.26401 |
Structure solution method | MOLECULAR REPLACEMENT |
Starting model (for MR) | PDB ID 4LL1 |
RMSD bond length | 0.022 |
RMSD bond angle | 2.148 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | MOLREP |
Refinement software | REFMAC (5.2.0019) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.800 |
High resolution limit [Å] | 2.700 | 2.700 |
Number of reflections | 24910 | |
Completeness [%] | 99.9 | 99.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 294.15 | 0.16M tri-sodium citrate, 16% PEG3350, pH 6.5, VAPOR DIFFUSION, SITTING DROP, temperature 294.15K |