4LHM
Thymidine phosphorylase from E.coli with 3'-azido-3'-deoxythymidine
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SPRING-8 BEAMLINE BL41XU |
Synchrotron site | SPring-8 |
Beamline | BL41XU |
Temperature [K] | 100 |
Detector technology | CCD |
Collection date | 2012-05-23 |
Wavelength(s) | 0.8 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 130.762, 130.762, 67.057 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 14.000 - 1.520 |
R-factor | 0.15537 |
Rwork | 0.153 |
R-free | 0.19578 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.008 |
RMSD bond angle | 1.250 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | PHASER |
Refinement software | REFMAC (5.7.0029) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 20.000 |
High resolution limit [Å] | 1.520 |
Number of reflections | 84887 |
Completeness [%] | 99.8 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | COUNTER-DIFFUSION | 298 | COUNTER DIFFUSION, temperature 298.0K |