4LGK
X-ray structure of the adduct between hen egg white lysozyme and Au2Phen, a dinuclear gold(III) complex with -dioxo bridges linking the two metal centers
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | ROTATING ANODE |
Source details | ENRAF-NONIUS FR571 |
Collection date | 2013-02-11 |
Wavelength(s) | 1.5418 |
Spacegroup name | P 43 21 2 |
Unit cell lengths | 77.435, 77.435, 37.191 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 25.350 - 1.960 |
R-factor | 0.21506 |
Rwork | 0.211 |
R-free | 0.30032 |
Structure solution method | FOURIER SYNTHESIS |
RMSD bond length | 0.021 |
RMSD bond angle | 1.938 |
Data reduction software | HKL-2000 |
Data scaling software | HKL-2000 |
Phasing software | CNS |
Refinement software | REFMAC (5.5.0109) |
Data quality characteristics
Overall | |
Low resolution limit [Å] | 26.800 |
High resolution limit [Å] | 1.960 |
Rmerge | 0.113 |
Number of reflections | 7204 |
Completeness [%] | 84.3 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 |